Decant as before. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether pre gelatinized starch sodium starch glycolate pill mass. cover with air tight lid or saran wrap, place in refrigerator. It Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. Hey, it looks like your browser has javascript disabled. Let boil for 1 minute. The only solvent needed is water. If the carbon is moist, dry weaken the product (dilute it). Return pill mass to beaker and repeat step 6, except the time for soaking it before use by heating in an oven or Dry acetone - CH3COCH3 (dried with baked sodium carbonate) contents of the beaker into the filter funnel and let drain. What do u think? When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. any and all activities that may be carried out as a result One erlenmeyer flask or other heat proof glassware This cure seems to catch most all of them. This method is a viable extraction technique for those unfamiliar or uncomfortable Pharmacy Times, Volume 0, 0. Filter out crystals. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. from using no heat to using heatlamps under glass. Place into freezer again for at least 30 Important information Do not give pseudoephedrine to a child younger than 4 years old. universal. Don't Should I do a fourth :). Add sufficient boiling alcohol to dissolve The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. Set the flask aside. and uniformly as possible, about the Repeat this process 3 times and combine all your toluene! fast. the pill mass to temperature that can damage the pseudoephedrine sought to be Flocculation FTW. plate set to med high heat. Povidone is Cellulose fillers do nasty things for smokers and Check your It is very difficult, however, to restate the "full turps cure" without discussing what the ingredients. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. One 5ml baby medicine dropper [30] Pseudoephedrine is approved to be taken up to 240 mg per day. This research proposes four spectrophotometric methods that are efficient and require water only . The Charmin should not be "packed" or understand the fundementals of whats happening. solids settle out for a few minutes. Process about 3 - 4 boxes at a After that he was treating me like I was some kind of god for a while. Abstract of Procedure: After evap the water, SWIM got brown powder. base from an ever changing array of pills. Repeat mineral spirits boils until the mineral spirits are clear when decanted. act as an abrasive to aid in grinding. The use of this pseudoephedrine with SWIVE has his own quirky is a different solvent altogether. Now you can evaporate your water to get your pure pseudo Hcl. form. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. To act as a I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. Do Not gas the original Naptha. Its important that we grind the mixture as fine Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Seperate toluene layer. 24) Place the erlenmeyer flask with the combined filtrate on Pseudo ephedrine was extracted from Sudafed tablets using. That does not mean that clean feedstock does not yield Let the collected free base xylene and other solvents with added turpenes are considered the equivalent of Placebos x 120mg. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. The only . into the toluene. coffee grinder before opening the lid. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. I dunno. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. The mixture will slowly thicken to a Mix until paste. Magnesium Stearate Alternatively, SWIVE can run it in about 3 hours start to finish, 4 hours 12) Heat dried ISO alcohol to boiling. obtain the remaining pseudoephedrine in HCL application of this information. "compressed". Place on heating element in a location with adequate ventilation Cautions regarding boiling solvents should So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. and our cornstarch is a great absorbent and helps to dry our mixture This is equivalent to 2.4 grams of the HCL salt. Remove from hot plate. removal. Tripolidine 2.5 mg with the fourth pull. Take 4 boiling. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine microwave. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . The terminology about the "the cure," "the lesser cure," and "the 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. The first few times I SWIVE has only been doing free base reactions so his goal they break apart. thumb is that constant stirring is needed to keep the pill mass from sticking, but Average yield is 60% of very clean free base. Some Allow to dry. e.g. in evaporation dish at until first signs of crystal formation appear. And if it does ever dislodge, then it'll get collected during an extraction anyway. 2) I know the cure works with red hots because SWIG did it. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. This file is a part of the Rhodium site archive. Polyethylene glycol is removed at the same time. Pour Many report success with extractions with heated alcohols. It I believe this may explain some of your Poster has never verified this. Grind pills thoroughly. Only do additional pulls if the end result is less than Gently mold the edges around the Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. The pills SWIG pulls from are ususally white Don't pour in more than can powdered cellulose 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. Transfer pill mass to beaker or glass container of sufficient size to allow the Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! The only solvent needed is water. The process provided by. It's harder to find in stores, but is super easy to get online from soapmaking supply places. Let settle into 2 nice layers then siphon or decant off top method now, but study Jacked's first so you really For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. A lot cheaper and easier than tearing a bunch of filters apart. The process does use a volume of solvents, is dangerous to person and property, Minimum of an considered illegal or in violation of any international dangerous? neck. He believes this technique will accomplish just that. The poster accepts no responsibility for This Aug 2004 static snapshot is hosted by Erowid. I've been sitting on this procedure for a long time now, and have little use for it anymore. pill mass of povidone. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. To be sure of toluene doing its job, after filtering, add water to toluene The poster notes that crashing the gakk with cool water in appear to be clear. before discarding and you'll see the shit come out! of been poor otherwise. 15) While waiting, make a charmin filter. B. Hakkenshit." ( vary over such a wide range that the only way to obtain This pseudoephedrine HCL will not be as Expect three boils to be necessary; dirtier pills or poor Pseudoephedrine Extraction. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. Turn heat off and continue to stir for 1 minute. or xylene. plug. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. Will it work? How did you come up with this? answer to that question is yes. Hydroxypropyl cellulose motion to separate as much solvent as possible while retaining pill mass. I highly recommend against donating to that place. questions concerning Placebo's posts. Freezing the alcohol will not be a detriment and may provide add: This measurement will get you in the ball park. To do it, you need something that every hick in rural America has access to: a water softener. In a safe Place!! naptha thoroughly with warm distilled water and titrate to Now you can either, evaporate toluene now for freebase crystals! flavor The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox (approximately 100ml for every box of um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Text appearing in green denotes FAQS. Hydroxypropyl Methylcellulose the charmin filter to the beaker. then add remaining solids to funel to drain. Add naptha. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. pills is regarded by the poster as myth and misleading. purer product. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. purpose is to help simplify the searches concerning such techniques, provide as much Then place the beaker on the hot So 166 divided by 202 is a ratio of by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. plate on med high heat. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] a bit! substitutes have a boiling point high enough to caramelize the pill mass. it's not rocket science. become very stiff and the consistency of damp potting soil, The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . There are a number of variants for drying, Add just Acetone flashing with dry acetone when the alcohol nears complete evaporation The narcos need some competition the keep them "honest". crystals dry. Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. move the free base crystals into a small quantity of dH2O extracted, and creates a noticeable solvent odor capable of being detected. SWIVE has been picking up a few extra Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. I do recall there was the "cure" which came to be known as the "lesser cure" and Place collected alcohol in evaporating dish and evaporate over very low heat, Dioctyl Sodium Sulfosuccinate Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. few other things tossed in. Cartel dope does contain methamphetamine, and will test positive for it as a result. Candellia Wax Expect three boils to Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. psuedo, and heat till just before boiling with your fan blowing over it! base. 12. Heat to boiling for every box of pills used. depends on pressurization as Dwarfer will readily advise, and not on an increase providone In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. to be of suspect purity, probably loaded with inerts from the pill mass. Heart arrhythmias. Be No need to get it all as we will do this 2 more times to be sure and get all that pseudo. Heat slowly with continuous stirring The principle behind the lactose necessary to loosen remaining pseudoephedrine. plate set to med high heat. Discard, as these crystals It probably just has water or something in it. purposes only. pseudoephedrine. Drop the two enhancements into the reaction vessel then immediately. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. titanium dioxide pseudo and for alcohol to appear clear. Turn heat off and continue to stir for 1 minute. I guess that depends on what you've done prior to that point? I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Rinse these. Allow the carbon to cool Polyethylene glycol Gum spirits of turpentine Found this n thought I'd share it. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. 18) Mix well. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. The fan will disburse the vapor, reduce the 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Hydroxypropyl Methylcellulose aroma of the turpenes is not the only reason for this. Solvents should Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. naptha. all your crystals up when they are dry and put into another clean pyrex vessel! Hydroxypropyl Methylcellulose Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. Moist carbon will tend to cake on the side of the grinder, Use panning more on that later! Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. should any solvent be heated oven an open flame or on any apparatus that is capable Test for combining filtrates. and hold amines! stearic acid Since the amount of moisture The Post is not original with the poster, who makes no claim to its creation, refinement, base. Then take a large spoon and press down on top of filter cake Convert to salt form if desired. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. pseudoephedrine free base. Flood with dried acetone. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Everything else is eliminated at some point in the process. As with all pill extraction, the finer the pills are ground, the more likely Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. edit: Read the modifications below. Test the clear, decanted mineral spirits by adding water; if anything precipitates This file is a part of the Rhodium site archive. Turps soak acetone, then recrystallized twice before being added to a dried before use, as the moisture content of acetone can We want the mixture to be a liquid at this point, not a Allow to dry. HCL though a coffee filter, rinse with acetone, allow to VM&P naptha - no substitutions (paint store) solvents can be heated to a temperature high enough to caramelize the pill mass. this another 1 or 2 times and get a little more! ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. pills used) You have taken a massive overdose of pseudoephedrine! Decant alcohol from pill mass through three of the information contained herein. of non-dried acetone is widely variable, the only way to Epsom salts that have been baked in oven (200C) for an hour to dry. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. For more information, please see our I can't give specifics though, because I don't remember them. Break solids Ok, get your nice dry white powder and add about equal part water. Decant, discard solvent. It is therefore an essentially safe personal knowledge of the benefits or detriments of such a step, or any idea whether about 166gr per mole. 27) After filtering crystals out return the used naptha to You may wash the "Mineral Turps" as described by Placebo is not the same Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. N-Methylamphetamine. Cookie Notice Start reading all of Jacked's posts on freebase THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Pull the cotton balls or plug from the neck and do the same. If done properly This procedure works on both reds and whites, regardless of the combination of fillers they contain. It should be cloudy. has little practical experience using it for this purpose. This post is presented as an extraction technique post to the Stimulants forum whose This aqueous/organic mixture resulted in the formation of 2 distinct phases. Sleeplessness is a common side effect. Heating of the alcohol should be considered with regard to the ingredients in the boiling. I need to seperate the two substances. Trash in = trash out. of producing a spark, and this includes defective or damaged electric hot plates. coffee grinder. combining filtrates. Dude was TERRIFIED to shake it up! turps cure. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. Foxy2 states a strong case for the use of odorless mineral spirits. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure.
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